Sonochemical Synthesis of Nano-structured Lead(II) Coordination Polymer with 2-Aminonicotinic Acid: Thermal, Structural and X-ray Powder Diffraction Studies
Identifieur interne : 000B08 ( Main/Exploration ); précédent : 000B07; suivant : 000B09Sonochemical Synthesis of Nano-structured Lead(II) Coordination Polymer with 2-Aminonicotinic Acid: Thermal, Structural and X-ray Powder Diffraction Studies
Auteurs : Ali Morsali [Iran] ; Akram Panjehpour [Iran] ; Sang Woo Joo [Corée du Sud]Source :
- Journal of Inorganic and Organometallic Polymers and Materials [ 1574-1443 ] ; 2012-11-01.
English descriptors
Abstract
Abstract: A new one-dimensional crystalline and nano-structured Pb(II) coordination polymer, [Pb(2-anc)2(NO3)2] n (1) {2-Hanc = 2-aminonicotinic acid}, were synthesized via heat gradient and sonochemical methods. The new produced nano-structure was characterized by scanning electron microscopy, X-ray powder diffraction, IR spectroscopy, and elemental analyses. Structural characterization by single crystal X-ray diffraction exhibits two-dimensional polymeric units for compound 1. Thermal stability of nano and bulk samples of compound 1 were studied and compared. PbO nano-particles was then obtained via calcination of nano-compound 1 at high and low temperatures. The calcinations result demonstrates that compound 1 may be suitable precursor for the preparation of nanoscale lead(II) oxide without need for special conditions like high temperature, long times and pressure control.
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DOI: 10.1007/s10904-012-9771-z
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Box 14155–4838, Tehran</wicri:regionArea><wicri:noRegion>Tehran</wicri:noRegion></affiliation><affiliation wicri:level="1"><country wicri:rule="url">Iran</country></affiliation></author><author><name sortKey="Panjehpour, Akram" sort="Panjehpour, Akram" uniqKey="Panjehpour A" first="Akram" last="Panjehpour">Akram Panjehpour</name><affiliation wicri:level="1"><country xml:lang="fr">Iran</country><wicri:regionArea>Department of Chemistry, Payame Noor University, Mashhad</wicri:regionArea><wicri:noRegion>Mashhad</wicri:noRegion></affiliation></author><author><name sortKey="Joo, Sang Woo" sort="Joo, Sang Woo" uniqKey="Joo S" first="Sang Woo" last="Joo">Sang Woo Joo</name><affiliation wicri:level="1"><country xml:lang="fr">Corée du Sud</country><wicri:regionArea>Center for Research Facilities, Yeungnam University, Gyongsan</wicri:regionArea><wicri:noRegion>Gyongsan</wicri:noRegion></affiliation><affiliation wicri:level="1"><country wicri:rule="url">Corée du Sud</country></affiliation></author></analytic><monogr></monogr><series><title level="j">Journal of Inorganic and Organometallic Polymers and Materials</title><title level="j" type="abbrev">J Inorg Organomet Polym</title><idno type="ISSN">1574-1443</idno><idno type="eISSN">1574-1451</idno><imprint><publisher>Springer US; http://www.springer-ny.com</publisher><pubPlace>Boston</pubPlace><date type="published" when="2012-11-01">2012-11-01</date><biblScope unit="volume">22</biblScope><biblScope unit="issue">6</biblScope><biblScope unit="page" from="1341">1341</biblScope><biblScope unit="page" to="1349">1349</biblScope></imprint><idno type="ISSN">1574-1443</idno></series></biblStruct></sourceDesc><seriesStmt><idno type="ISSN">1574-1443</idno></seriesStmt></fileDesc><profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Coordination polymer</term><term>Crystal structure</term><term>Lead(II) oxide</term><term>Nano-structure</term></keywords></textClass><langUsage><language ident="en">en</language></langUsage></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">Abstract: A new one-dimensional crystalline and nano-structured Pb(II) coordination polymer, [Pb(2-anc)2(NO3)2] n (1) {2-Hanc = 2-aminonicotinic acid}, were synthesized via heat gradient and sonochemical methods. The new produced nano-structure was characterized by scanning electron microscopy, X-ray powder diffraction, IR spectroscopy, and elemental analyses. Structural characterization by single crystal X-ray diffraction exhibits two-dimensional polymeric units for compound 1. Thermal stability of nano and bulk samples of compound 1 were studied and compared. PbO nano-particles was then obtained via calcination of nano-compound 1 at high and low temperatures. The calcinations result demonstrates that compound 1 may be suitable precursor for the preparation of nanoscale lead(II) oxide without need for special conditions like high temperature, long times and pressure control.</div></front></TEI><affiliations><list><country><li>Corée du Sud</li><li>Iran</li></country></list><tree><country name="Iran"><noRegion><name sortKey="Morsali, Ali" sort="Morsali, Ali" uniqKey="Morsali A" first="Ali" last="Morsali">Ali Morsali</name></noRegion><name sortKey="Morsali, Ali" sort="Morsali, Ali" uniqKey="Morsali A" first="Ali" last="Morsali">Ali Morsali</name><name sortKey="Panjehpour, Akram" sort="Panjehpour, Akram" uniqKey="Panjehpour A" first="Akram" last="Panjehpour">Akram Panjehpour</name></country><country name="Corée du Sud"><noRegion><name sortKey="Joo, Sang Woo" sort="Joo, Sang Woo" uniqKey="Joo S" first="Sang Woo" last="Joo">Sang Woo Joo</name></noRegion><name sortKey="Joo, Sang Woo" sort="Joo, Sang Woo" uniqKey="Joo S" first="Sang Woo" last="Joo">Sang Woo Joo</name></country></tree></affiliations></record>Pour manipuler ce document sous Unix (Dilib)
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